Sleep Tight - S3-E16
Audio problem: At the end of the episode when Holtz jumps into the dimensional rift with Connor, we hear Angel yell "no" twice. But his lips don't move on either occasion.
Benediction - S3-E21
Audio problem: When Cordelia has her vision about the vampires at the bar, her lips don't match the words "Vampires, a gang of them".
Visible crew/equipment: When Angel is fighting the demon, you can see an obvious camera and two hands in the bottom right corner. (00:27:10)
Cordelia: You want I should distract him? Make with the nice-nice while you slip by?
Angel: Don't be stupid. I'm that guy and the most beautiful woman I've ever seen is making eyes at me? It's either a bachelor party or a scam.
Cordelia: What did you just call me?
Angel: I'm sorry. You're not stupid.
Cordelia: No, after that.
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Answer: Due to his epiphany, Angel basically had the 'true darkness' he worked so hard to reattain ripped away from him, like his soul was after sleeping with Buffy.