The Enterprise Incident - S3-E2
Plot hole: Despite the Romulan ships keeping a close watch on the Enterprise, when they beam the disguised Cpt Kirk over to the Romulan vessel it goes undetected.
Plot hole: If diverting the asteroid was so important, what was the crew doing on the planet to begin with?
Is There in Truth No Beauty? - S3-E5
Plot hole: When the Medusan Ambassador Kollos and Dr. Jones materialize, the latter is wearing a protective visor and Mr. Spock can see that. Spock then mistakenly addresses Dr. Jones as Ambassador Kollos. Spock's suddenly illogical mistake seems odd: why should the Ambassador need to wear a visor? Shortly after, why do both Jones and Spock wear visors while carrying the Ambassador's still closed gasket to his cabin? (00:01:45)
The Empath - S3-E12
Plot hole: Spock calculates that it will take 72 hours for the solar flare to pass, and Kirk orders the Enterprise out of the area. 3 days is a long time to go without food or water, and as the station is deserted as far as they know, there'd be no way to supply themselves, but the Enterprise leaves without a second thought.
Plot hole: The law officer who arrests Kirk recalls hearing Kirk call the "spirit" Bones. But he wasn't there when Kirk spoke to McCoy. He rushed into the scene several minutes later. If he's lying, how would he know that Kirk used the name Bones? He wasn't there to hear it. Even if he had been, Kirk did not refer to McCoy as Bones in that conversation. (00:10:50 - 00:19:50)
Answer: Kirk was getting his physical and Dr. McCoy probably turned off communications, because if he hadn't, Kirk would have left and headed straight for the bridge, leaving McCoy irritated.